反応 #1839

反応方程式

5-hydroxy-2-nitrobenzyl alcohol

isopropyl iodide

→

2-Nitro-5-(2-propyloxy)benzyl alcohol

反応条件

後処理

1. 1
   その他after purification over silica gel with n-heptane/ethyl acetate (3:2), 10.3 g of oily crude product

実験手順

10 g (60 mmol) of 5-hydroxy-2-nitrobenzyl alcohol were reacted with 7.0 ml (70 mmol) of isopropyl iodide analogously to Example 4a); after purification over silica gel with n-heptane/ethyl acetate (3:2), 10.3 g of oily crude product.

出典