反応 #1824307

反応方程式

copper(II) acetate

glycine

→

copper(II) glycinate

溶媒

methanol

methanol

反応条件

後処理

1. 1
   workup.STIRRINGAfter stirring for 2 hours at a falling temperature
2. 2
   その他the product precipitated
3. 3
   ろ過is filtered off
4. 4
   その他dried

実験手順

1.8 g (9.8 mmoles) of copper(II) acetate are dissolved in 100 ml of hot methanol and a solution of 1.5 g (20 mmoles) of glycine in 50 ml of methanol is added with stirring to the resulting solution. The solution turns cloudy under the effect of precipitated product. After stirring for 2 hours at a falling temperature, the product precipitated is filtered off and dried. Yield: 2.5 g (96% of the theoretical), Mp.:>210° C.

出典