反応 #1810806

ord-26d5dd4e7ab34ea3bd1bf925f10025a1

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The mixture obtained
  2. 2
    その他solvent is evaporated

実験手順

0.90 g of Methyl-isothiocyanate are added to a solution of 1.74 g of trans-4-dimethylamino-cyclohexanamine in 50 ml of EtAc. The mixture obtained is stirred at RT, solvent is evaporated and 1-(4-dimethylaminocyclohexyl)-3-methyl-thiourea is obtained.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07485632B2uspto-grants-2009_02