反応 #1810794

反応方程式

ethyl 3-hydroxybutyrate

ethyl 4-azido-3-hydroxybutyrate

→

ethyl (S)-4-azido-3-hydroxybutyrate

収率 80.2%

反応条件

実験手順

Instead of ethyl 3-hydroxybutyrate used in Example 1, ethyl 4-azido-3-hydroxybutyrate was used. The reaction was carried out for 1 hour and ethyl (S)-4-azido-3-hydroxybutyrate (80.2% e.e) was obtained at 83.5% conversion.

出典