反応 #1810686
ord-e6a02c105a404939b46c9679e6cdda00
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
The title compound was prepared by the procedure of Example 1 starting with (A) of Example 1 (8.0 g, 25 mmol) and using imidazole in place of dibutylamine to produce 2.1 g (24% yield) of the free base of the title compound which was converted to the HCl salt, mp 158°-159° C. IR(KBr): 3400, 1600 cm-1. MS: 346(MH+). 1H NMR (CD3OD): δ 9.09 (s, 1H), 7.82-6.81 (m, 12H), 4.51 (t, J=5.4 Hz, 2H), 4.08 (t, J=5.1 Hz, 2H), 2.41 (m, 2H).