反応 #1797481

反応方程式

CF3OCF(CF3)CF2OCF═CF2

isopropanol

→

CF3OCF(CF3)CF2OCFHCF2C(CH3)2OH

反応条件

後処理

1. 1
   その他at 75° C
2. 2
   その他The resulting product reaction mixture
3. 3
   workup.DISTILLATIONwas distilled
4. 4
   その他=161-166° C.

実験手順

CF3OCF(CF3)CF2OCFHCF2C(CH3)2OH was prepared by the reaction of CF3OCF(CF3)CF2OCF═CF2 (52.9 g, 0.16 mol) with isopropanol (202 g, 3.37 mol) using LUPEROX 575 (11.4 g) as free radical initiator at 75° C. The resulting product reaction mixture was distilled and the distillation fraction of b.r.=161-166° C. used in the next step.

出典