反応 #1797478
ord-49530173db4a46ca88018fc46e3407e0
反応方程式
chlorpheniramine maleate
→
Chlorpheniramine
溶媒
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1洗浄the product washed with USP water
- 2その他The wet cake was dried
- 3ろ過sieved through a US Std #30 mesh screen
実験手順
Chlorpheniramine polistirex was prepared by mixing 3.12 kg of chlorpheniramine maleate with 26.00 kg of ion-exchange resin particles (AMBERLITE IRP69; US Std. Mesh #100-#400) suspended in USP water at about 30° C. The resulting suspension was centrifuged and the product washed with USP water. The wet cake was dried and sieved through a US Std #30 mesh screen. The chlorpheniramine content of the dried product was equivalent to approximately 11% by weight.