反応 #1771993
ord-40794a691015423f8f8e6dd4b847146a
反応方程式
Boc-4-phenylproline
→
product
収率 95.4%
Boc-4-cyclohexylproline
収率 95.4%
溶媒
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1ろ過The mixture was filtered
- 2濃縮concentrated
実験手順
A solution of the commercially available Boc-4-phenylproline (750 mg) and 5% Rh on carbon (750 mg) in methanol (15 mL) was hydrogenated at 50 psi for 24 hours. The mixture was filtered and concentrated to give 730 mg of product.