反応 #1771992

反応方程式

N-tertbutoxycarbonyl-4-allyl-4-methylproline

→

N-tert-butoxycarbonyl 4-propyl-4-methylproline

溶媒

methanol

反応条件

後処理

1. 1
   ろ過The mixture was filtered
2. 2
   濃縮concentrated

実験手順

A solution of N-tertbutoxycarbonyl-4-allyl-4-methylproline (400 mg, 1.48 mmol) (see Example II Step 4) and 10% Pd on carbon (400 mg) in methanol (20 mL) was hydrogenated at 50 psi for 4 hours. The mixture was filtered and concentrated.

出典