反応 #1771990
ord-56238b79bf8e4876a8c816dff94dc2f6
反応方程式
tert-butyl N-tert-butoxycarbonyl-4,4-dimethylproline
→
4,4-Dimethylproline
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1濃縮The solution was concentrated
- 2その他dried under high vacuum
- 3その他taken to the next step without further purification
実験手順
A solution of tert-butyl N-tert-butoxycarbonyl-4,4-dimethylproline in dichloromethane (5 mL) and trifluoroacetic (5 mL) was stirred at room temperature for five hours. The solution was concentrated, dried under high vacuum and taken to the next step without further purification.