反応 #1771636

ord-9cf21c2c105241fc92d571a2f280e35b

反応方程式

CCOc1ccc(O)c(F)c1F
2,3-difluoro-4-ethoxyphenol
CCCCCCC[Si]1(c2ccccc2)CCC(CBr)CC1
4-bromomethyl-1-n-heptyl-1-phenyl-1-silacyclohexane
CCCCCCC[Si@H]1CC[C@H](COc2ccc(OCC)c(F)c2F)CC1
trans-4-(2,3-difluoro-4-ethoxyphenyloxymethyl)-1-n-heptyl-1-silacyclohexane

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他obtaining the intended compound

実験手順

The general procedure of Example 9 was repeated using 2,3-difluoro-4-ethoxyphenol and 4-bromomethyl-1-n-heptyl-1-phenyl-1-silacyclohexane, thereby obtaining the intended compound.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05641430uspto-grants-1997_06