反応 #1730514

ord-a99cdb66714644ba8381f1cfe23b712b

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他Methanol is removed by fractionated distillation
  2. 2
    その他The resulting aqueous solution is used as an emulsifier in the polymerization of fluorinated olefins

実験手順

The calculated yield was 59% based on total PPVE used; 70% based on converted PPVE. The ester is converted to the ammonium salt by reaction with aqueous ammonia. Methanol is removed by fractionated distillation. The resulting aqueous solution is used as an emulsifier in the polymerization of fluorinated olefins.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08119750B2uspto-grants-2012_02