反応 #1722967

反応方程式

Pentafluorobenzenesulfonyl chloride

tetramethylammonium hydroxide

→

tetramethylammonium pentafluorobenzenesulfonate

溶媒

methanol

反応条件

実験手順

Pentafluorobenzenesulfonyl chloride (25 g) was dissolved in 100 ml of methanol under ice cooling, and 100 g of a 25% aqueous solution of tetramethylammonium hydroxide was slowly added thereto, followed by stirring at room temperature for 3 hours. Thus, a solution of tetramethylammonium pentafluorobenzenesulfonate was obtained. This solution was used for salt interchange with a sulfonium salt and an iodonium salt.

出典