反応 #171129

ord-01b081e27a914390b17b8bb8f541974c

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他yielding a polymer with a glass transition temperature of 145° C

実験手順

Similar to Example 51, with the following exception: 3.390 g (3.46×10−2 mol) α-methylene-γ-butyrolactone and 1.075 g (8.39×10−3 mol) n-butyl acrylate were used in the monomer mixture, yielding a polymer with a glass transition temperature of 145° C. Comparison to the Fox equation suggests the statistical copolymer contains approximately 11% n-butyl acrylate repeat units.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08846817B2uspto-grants-2014_09