反応 #1702019

反応方程式

tris[2-(2-methoxyethoxy)-ethyl]amine

2-acrylamido-2-methyl-1-propanesulfonic acid

→

2-acrylamido-2-methyl-1-propanesulfonic acid-ammonium salt

収率 99.0%

反応条件

後処理

1. 1
   その他A nitrogen purged 50 ml schlenk flask
2. 2
   workup.DISSOLUTIONuntil completely dissolved
3. 3
   workup.DISSOLUTIONTotal dissolution
4. 4
   その他was used immediately without further purification

実験手順

A nitrogen purged 50 ml schlenk flask was charged with freshly distilled tris[2-(2-methoxyethoxy)-ethyl]amine (1.69 g, 5.24 mmol) and 2-acrylamido-2-methyl-1-propanesulfonic acid (AMPS) (1.09 g, 5.24 mmol) and stirred at ambient temperature for 8 hr or until completely dissolved. Total dissolution completes formation of the AMPS-ammonium salt monomer as a transparent light amber oil in a 99% yield which was used immediately without further purification.

出典