反応 #1687647

反応方程式

( 3 )

4-acetoxy-2-fluoro-1-(1-ethylpropyloxycarbonyl)benzene

benzylamine

→

4-hydroxy-2-fluoro-1-(1-ethylpropyloxycarbonyl)benzene

溶媒

ether

ethanol

反応条件

後処理

1. 1
   洗浄the diluted mixture was washed with diluted hydrochloric acid
2. 2
   乾燥with water and dried over magnesium sulfate

実験手順

0.5 Gram of the compound obtained in the above (3) was dissolved in 30 ml of ethanol, and 1.5 g of benzylamine was added dropwise thereto. Further, the mixture was stirred at room temperature for one day and diluted with 300 ml of ether, and the diluted mixture was washed with diluted hydrochloric acid and then with water and dried over magnesium sulfate.

出典