反応 #1687635

反応方程式

fumarate

88

5-Methyl-2-(3-pyridyl)-thiazole

→

title compound

5-Methyl-2-(1-methyl-1,2,5,6-tetrahydro-3-pyridyl)-thiazole

反応条件

後処理

1. 1
   その他The crude free base obtained

実験手順

The title compound was prepared from 88 (2.2 g, 0.013 mol) by the procedure described in Example 49. The crude free base obtained, 89, was converted to the title fumarate, 90. Yield: 0.8 g (0.0032 mol, 25%). M.P. 159°-160° C. Anal. (C12H16N2O2S)C, H, N.

出典