反応 #167496

ord-a4ea7b3575bb42a39ffe1cfca97286af

反応方程式

OCc1ccccc1-c1cccc2ccccc12
Compound 13
OCc1ccccc1-c1cccc2ccccc12
[(naphthyl)phenyl]methanol
[Mg]
magnesium
Cc1ccc(Br)cc1
p-bromotoluene
O=C(c1ccccc1)c1ccccc1
benzophenone
Cc1ccc(CO)c(-c2ccccc2)c1-c1ccccc1
title compound
Cc1ccc(CO)c(-c2ccccc2)c1-c1ccccc1
[diphenyl(4-methylphenyl)]methanol

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他to react with the reagent

実験手順

With the same method as for Compound 13, a Grignard reagent was prepared from magnesium (Wako Pure Chemical Industries, Ltd.) and p-bromotoluene (Wako Pure Chemical Industries, Ltd.), and benzophenone (Wako Pure Chemical Industries, Ltd.) was allowed to react with the reagent, to thereby obtain the title compound. m.p. 68-71° C.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08846012B2uspto-grants-2014_09