反応 #167199
ord-c3685adb3002404b87876588e082935b
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
2-[(Z)-Ethylimino]-3-(2,3-dimethylphenyl)-thiazolidin-4-one is prepared following Method B and starting from 2,3-dimethylaniline, chloroacetyl chloride and ethylisothio-cyanate. LC-MS: tR=0.66 min, [M+1]+=249, 1H NMR (CDCl3): δ 7.24-7.19 (m, 2H), 7.00-6.96 (m, 1H), 4.01 (s, 2H), 3.45-3.27 (m, 2H), 2.34 (s, 3H), 2.05 (s, 3H), 1.16 (t, J=7.0 Hz, 3H).