反応 #1668107

ord-498dea4f845a4e57837ab697b1c5b977

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Following the procedure described in 1c above, N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride was catalytically hydrogenated in aqueous solution at 70°-75°C. and at 600 pounds per square inch in the presence of a 5 per cent platinum sulfide on charcoal mixture to obtain N,N-dimethyl-N-(4-aminophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US03935182uspto-grants-1976_01