反応 #166031

反応方程式

3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid

intermediate 1

3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid

2,2-diethoxy-ethylamine

→

N-(2,2-diethoxyethyl)-3-[(2-fluoro-4-iodophenyl)amino]isonicotinamide

反応条件

後処理

1. 1
   その他LC/MS [5.51 min; 474 (M+1)]

実験手順

N-(2,2-diethoxyethyl)-3-[(2-fluoro-4-iodophenyl)amino]isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.33 mmol of 3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid (intermediate 1) and 0.5 mmol of 2,2-diethoxy-ethylamine. LC/MS [5.51 min; 474 (M+1)]

出典