反応 #165990

ord-8d863f0e6d2c4898bf427c22ab7065eb

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他LC/MS [8.99 min; 455 (M+1)]

実験手順

N-azepan-1-yl-3-[(2-fluoro-4-iodophenyl)amino]isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.45 mmol of 3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid (intermediate 1) and 6.2 mmol of azepan-1-ylamine. LC/MS [8.99 min; 455 (M+1)]

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08841459B2uspto-grants-2014_09