反応 #1635

反応方程式

n-hexylphosphinic acid, n-butyl ester

paraformaldehyde

→

title compound

n-Hexylhydroxymethylphosphinic acid, n-butyl ester

反応条件

後処理

1. 1
   その他Purification by chromatography
2. 2
   洗浄eluting with dichloromethane containing 5% methanol
3. 3
   その他gave an oil

実験手順

The title compound was prepared from n-hexylphosphinic acid, n-butyl ester and paraformaldehyde according to the method described in Procedure 31. Purification by chromatography, eluting with dichloromethane containing 5% methanol, gave an oil.

出典