反応 #163487
ord-c829ad5c8c004e5c85e2ea643e0ba45b
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1ろ過filtered
- 2濃縮concentrated
実験手順
To a suspension of 1-fluoro-2-methylpropan-2-amine hydrochloride (ABCR) (2 g, 15.7 mmol), anhydrous magnesium sulfate (3.77 g, 31.4 mmol) and potassium carbonate (2.17 g, 15.68 mmol) in dichloromethane (100 mL) was added drop wise hexanal (1.93 mL, 15.7 mmol) at 0° C. The reaction mixture was stirred for 10 h at room temperature, then filtered and concentrated to obtain the title compound as a pale yellow liquid.