反応 #161187

ord-73910f44ef1f446f9ad354ba6ba5527f

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

2-tert-Butyl-4-(3-ethoxyphenyl)-5-aminophenol (C-16) was synthesized following the general scheme above starting from 2-tert-butyl-4-bromo-5-nitrophenol (C-14-a) and 3-ethoxyphenyl boronic acid. HPLC ret. time 2.77 min, 10-99% CH3CN, 5 min run; ESI-MS 286.1 m/z (MH+).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08829204B2uspto-grants-2014_09