反応 #1611734

ord-e5a0c3f4a8d247e2af21eb92fa687289

反応方程式

CC(C)(C)CCBr
1-bromo-3,3-dimethylbutane
CC(=O)c1cc(O)cc(O)c1
1-(3,5-Dihydroxyphenyl)ethanone
O=O
O2
BrC1CCCCC1
cyclohexylbromide
CCOc1cc(OCCC(C)(C)C)cc(C(C)=O)c1
title compound
CCOc1cc(OCCC(C)(C)C)cc(C(C)=O)c1
1-[3-(3,3-Dimethylbutoxy)-5-ethoxyphenyl]ethanone

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

1-(3,5-Dihydroxyphenyl)ethanone (3.0 g) was converted analogously to O2.031. Instead of cyclohexylbromide, however, 1-bromo-3,3-dimethylbutane was used. After chromatography, 960 mg of the title compound were obtained.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US09079906B2uspto-grants-2015_07