反応 #161119

反応方程式

6-nitroindole

iodo-acetic acid ethyl ester

→

(6-Amino-1H-indol-3-yl)-acetic acid ethyl ester

溶媒

CH3CN

反応条件

後処理

1. 1
   その他Overall yield (24%)

実験手順

(6-Amino-1H-indol-3-yl)-acetic acid ethyl ester (B-17) was synthesized following the general scheme above starting from 6-nitroindole and iodo-acetic acid ethyl ester. Overall yield (24%). HPLC ret. time 0.95 min, 10-99% CH3CN, 5 min run; ESI-MS 219.2 m/z (MH+).

出典