反応 #160960

反応方程式

5-bromo-6-chloro-nicotinic acid

4-(perfluoroethoxy)aniline

→

title compound

5-Bromo-6-chloro-N-(4-(perfluoroethoxy)phenyl)nicotinamide

反応条件

後処理

1. 1
   その他to afford an off-white crystalline solid

実験手順

The title compound was prepared in an analogous fashion to that described in Stage 9.3 using 5-bromo-6-chloro-nicotinic acid and 4-(perfluoroethoxy)aniline to afford an off-white crystalline solid. HPLC (Condition 4) tR=6.73 min, UPLC-MS (Condition 3) tR=1.30 min, m/z=443.1 [M−H]−.

出典