反応 #1596995

ord-84289a27ef1a4e41b17689cb80d0be1e

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他in Synthesis Example 1

実験手順

By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (2.00 g, 13.0 mmole) and 4-nitrobenzyl bromide (3.38 g, 15.6 mmole), 2.90 g (79% yield) of 5-(4-nitrobenzyl)aminosalicylic acid was obtained as a pale yellow solid.:mp 211-212° C.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08211877B2uspto-grants-2012_07