反応 #1577824

ord-40214ff4ce0d4d03aa7760f498a76e0b

反応方程式

c1scc2c1OCCO2
c1scc2c1OCCO2
→
CC1(C)OB(c2scc3c2OCCO3)OC1(C)C
CC1(C)OB(c2scc3c2OCC
収率 85.0%

反応物

c1scc2c1OCCO2
c1scc2c1OCCO2
CAS: 126213-50-1

試薬

CC1(C)CCCC(C)(C)[NH+]1c1ccccc1[B-](F)(F)F
CC1(C)CCCC(C)(C)[NH+]1c1ccccc1
CAS: 1892583-35-5
CC1(C)OBOC1(C)C
CC1(C)OBOC1(C)C
CAS: 25015-63-8

反応条件

温度
80°CELSIUS

出典

DOI: 10.1021/jacs.7b08143Borylation dataset from Roche