反応 #156609

ord-f20b44f76d09419c9373313e65a961cf

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The product with the molecular weight of 216.30 (C13H12OS) was obtained in this way

実験手順

5-Bromo-3-methylthiophene-2-carbaldehyde (Spinelli, D. et al., J. Chem. Soc. Perkin Trans. 2, 1972, (12), 1866-9) was reacted with 4-methylphenylboronic acid by method J. The product with the molecular weight of 216.30 (C13H12OS) was obtained in this way; MS (ESI): 217 (M+H+).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08822495B2uspto-grants-2014_09