反応 #1552043
ord-5457b3292eac4bc197a3beacfcc105ba
反応方程式
N-methoxy-acrylamide
chloroformic acid vinyl ester
→
title compound
N-Methoxy-N-propenoylcarbamic acid vinyl ester
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他Purification by column chromatography on silica gel (PE:EE=9:1)
実験手順
The synthesis was carried out analogously to synthesis example 8 using N-methoxy-acrylamide and chloroformic acid vinyl ester. Purification by column chromatography on silica gel (PE:EE=9:1) yielded 1.6 g (91% of th.) of the title compound as a colorless liquid.