反応 #1552022

反応方程式

iodine monochloride

1-chloro-9-iodoperfluorononane

perfluorocyclopropane

1-chloro-11-iodoperfluoroundecane

→

1-chloro-3-iodoperfluoropropane

反応条件

後処理

1. 1
   その他can be obtained

実験手順

As for a compound in which n is 9 or 11 in formula (22), 1-chloro-9-iodoperfluorononane (22-4) or 1-chloro-11-iodoperfluoroundecane (22-5) can be obtained by allowing iodine monochloride to react with commercially available perfluorocyclopropane (53) at a high temperature to obtain 1-chloro-3-iodoperfluoropropane (54), and then allowing 1-chloro-3-iodoperfluoropropane (54) to react with tetrafluoroethylene (51) under high temperature and pressurized conditions.

出典