反応 #1534287

ord-7bad8b82b66346d480649e5c185fe4b1

反応方程式

O=P([O-])([O-])OP(=O)([O-])OP(=O)([O-])[O-].[Na+].[Na+].[Na+].[Na+].[Na+]
sodium tripolyphosphate
→
O.O.O.O.O.O.O=P([O-])([O-])OP(=O)([O-])OP(=O)([O-])[O-].[Na+].[Na+].[Na+].[Na+].[Na+]
sodium tripolyphosphate hexahydrate

反応物

O=P([O-])([O-])OP(=O)([O-])OP(=O)([O-])[O-].[Na+].[Na+].[Na+].[Na+].[Na+]
sodium tripolyphosphate

試薬

なし

溶媒

O
water
O
water
O
water
O
water

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    workup.ADDITIONwas added
  2. 2
    その他the product was dried in the rotary drum at temperatures of 50°-70° C.
  3. 3
    その他The temperature of the product being dried
  4. 4
    その他Drying

実験手順

While the drum was rotating at about 6 rpm, the water was sprayed onto the solids at the rate of about 50 ml/min. Spraying was stopped after each 50 ml portion of water was added and the bed of semi-moisturized sodium tripolyphosphate was thoroughly mixed with a large spatula. When the desired amount of water had been added, water addition was stopped and the product was dried in the rotary drum at temperatures of 50°-70° C. by blowing hot air from a heat gun into the rotary. The temperature of the product being dried was measured by a stainless steel thermometer stem placed in the tumbling bed of product. Drying was conducted for about one hour and generally provided a sodium tripolyphosphate hexahydrate product having a free moisture content of less than about 1 weight percent and a total moisture content of between 18 and 22 weight percent.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04315898uspto-grants-1982_02