反応 #1528417

ord-74357077942943cdbbbbc0e3ce23eaf7

反応方程式

O=C(NCC1(CC2CC2)CCN(S(=O)(=O)c2c[nH]nn2)CC1)c1ccc(Cl)cc1Cl
2,4-Dichloro-N-[4-(cyclopropylmethyl)-1-(1H-[1,2,3]triazole-4-sulfonyl)piperidin-4-ylmethyl]benzamide
O=C([O-])[O-].[K+].[K+]
Potassium carbonate
CI
methyl iodide
Cn1cc(S(=O)(=O)N2CCC(CNC(=O)c3ccc(Cl)cc3Cl)(CC3CC3)CC2)nn1
2,4-Dichloro-N-[4-(cyclopropylmethyl)-1-(1-methyl-1H-[1,2,3]-triazole-4-sulfonyl)piperidin-4-ylmethyl]-benzamide

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

2,4-Dichloro-N-[4-(cyclopropylmethyl)-1-(1H-[1,2,3]triazole-4-sulfonyl)piperidin-4-ylmethyl]benzamide (472 mg, 1.0 mmol) was dissolved in N,N-dimethylformamide (5 mL). Potassium carbonate (276 mg, 2 mmol) and methyl iodide (81 μL, 1.3 mmol) were added and the mixture stirred at room temperature over night.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07655644B2uspto-grants-2010_02