反応 #1518

反応方程式

4-(6-decyloxy-2-naphthoyloxy)benzoic acid benzyl ester

hydrogen

→

4-(6-decyloxy-2-naphthoyloxy)benzoic acid

収率 97.5%

溶媒

THF

反応条件

後処理

1. 1
   ろ過filtered

実験手順

To 37.6 g (0.07 mol) of the 4-(6-decyloxy-2-naphthoyloxy)benzoic acid benzyl ester obtained in the first stage was added 3.76 g of 5% palladium/carbon, and further added 188 g of THF. Then, hydrogen gas was blown into the mixture. The resultant mixture was stirred overnight and filtered to obtain 30.6 g of 4-(6-decyloxy-2-naphthoyloxy)benzoic acid.

出典