反応 #1515623

反応方程式

1-methylnaphthalene

methacryloyl chloride

aluminium chloride

→

title compound

収率 58.1%

1-methyl-6-methacryloylnaphthalene

収率 58.1%

溶媒

dichloromethane

反応条件

後処理

1. 1
   workup.ADDITIONThe resultant was treated in the same manner

実験手順

1-methylnaphthalene (142 mg), methacryloyl chloride (110 mg), and aluminium chloride (160 mg) were reacted in dichloromethane (1.5 mL) at from −30° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (122 mg).

出典