反応 #1478591

反応方程式

acetophenone

hydrazine

→

oil

収率 69.0%

Acetophenone hydrazone

収率 69.0%

溶媒

ethanol

反応条件

後処理

1. 1
   温度The mixture is heated
2. 2
   温度to reflux temperature
3. 3
   その他the solvent is evaporated
4. 4
   洗浄The medium is washed with water (100 ml)
5. 5
   乾燥After drying over Na2SO4
6. 6
   その他the ether is evaporated off

実験手順

acetophenone (2.0 g, 16 mmol) is diluted in 16 ml of absolute ethanol and then hydrazine (2.3 ml, 48 mmol) is added. The mixture is heated to reflux temperature. After 2 h, the solvent is evaporated and the residue is taken up in ether (150 ml). The medium is washed with water (100 ml). After drying over Na2SO4, the ether is evaporated off. A pale yellow oil (1.5 g, 11 mmol, 69%) is obtained.

出典