反応 #1470428

反応方程式

1-hydroxy-2,2,6,6-tetramethyl-4-hydroxypiperidine

acetic acid

→

hydroxylamine

収率 59.1%

1-Hydroxy-2,2,6,6-tetramethyl-4-hydroxypiperidinium Acetate

収率 59.1%

溶媒

isopropanol

反応条件

実験手順

5.0 g (0.029 mol) 1-hydroxy-2,2,6,6-tetramethyl-4-hydroxypiperidine and 2.0 g (0.033 mol) acetic acid are recrystallized from 50 mL of isopropanol, yielding 4.0 g of the desired hydroxylamine salt as a white crystalline solid, mp 140-143° C.

出典