反応 #1470426

反応方程式

1-oxyl-2,2,6,6-tetramethyl-4-glycidyloxypiperidine

dimethylamine

→

title compound

収率 82.8%

1-Oxyl-2,2,6,6-tetramethyl-4-(2-hydroxy-3-dimethylaminopropoxy)piperidine

収率 82.8%

溶媒

water

反応条件

後処理

1. 1
   その他Water is then removed by vacuum distillation

実験手順

A mixture of 10.0 g (0.044 mol) of 1-oxyl-2,2,6,6-tetramethyl-4-glycidyloxypiperidine and 10 mL of 40% (ca. 0.091 mol) of dimethylamine (w/w) is dissolved in 100 mL of water and then stirred for 16 hours at ambient temperature. Water is then removed by vacuum distillation to leave 10 g of the title compound as a red oil.

出典