反応 #1465687
ord-c8cbaf41739b4dd5940d1fcb584e1d36
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1温度The mixture was maintained
- 2ろ過was then filtered
- 3その他The filtrate was dried under reduced pressure (133 Pa) overnight with the exclusion of light
- 4その他16.33 g (or a yield of 75%) of diphenyliodonium tetrakis(pentafluorophenyl)borate were thus recovered
実験手順
7.17 g (or 22.6 mmol) of diphenyliodonium chloride were dissolved in 300 ml of water in a 1,000 ml Erlenmeyer flask. 15.52 g (or 22.6 mmol) of lithium tetrakis(pentafluorophenyl)borate in solution in 250 ml of water were added dropwise. The mixture was maintained under stirring for 30 minutes and was then filtered. The filtrate was dried under reduced pressure (133 Pa) overnight with the exclusion of light. 16.33 g (or a yield of 75%) of diphenyliodonium tetrakis(pentafluorophenyl)borate were thus recovered.