反応 #1460654
ord-5ac03c4a0ee34554b5204a07009a273c
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他Formed clear solution
- 2ろ過is filtered
- 3その他evaporated to dryness
実験手順
88.54 g (0.200 mol) of di(pentafluorophenyl)chloroethoxysilane in Et2O is slowly added to solution of C6F5—Li (0.200 mol, 34.80 g, prepared in situ) in Et2O at −78° C. The solution is stirred for over night allowing it to warm up to room temperature. Formed clear solution is filtered and evaporated to dryness to result tri(pentafluorophenyl)ethoxysilane, (C6F5)3SiOEt.