反応 #1447117

ord-3ddd7d4e011440eb9d7c77cc15a78b39

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Following the procedure described for Example 1, step 2, treatment of a solution in DCM (0.090 M) of 4-chlorophenyl dichlorophosphate with L-alanine ethyl ester hydrochloride (1.0 eq.) and Et3N (2.0 eq.) provided the title compound as a colorless oil as a 1:1* mixture of diastereoisomers.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07879815B2uspto-grants-2011_02