反応 #1447094

反応方程式

Acetic anhydride

4-bromo-3-methoxy-phenylamine

→

N-(4-Bromo-3-methoxy-phenyl)-acetamide

溶媒

acetic acid

—

ice

反応条件

後処理

1. 1
   その他The precipitate is separated by filtration
2. 2
   洗浄washed with water
3. 3
   その他dried at 60° C.
4. 4
   その他to give the product

実験手順

Acetic anhydride (13 mL) is added to an ice-cold solution of 4-bromo-3-methoxy-phenylamine (25.0 g) in acetic acid (100 mL). The mixture is stirred for 1 h and then diluted with ice-cold water (500 mL). The precipitate is separated by filtration, washed with water and dried at 60° C. to give the product.

出典