反応 #1435710
ord-4cd34ebc3a174a06b6c043dac224b55d
反応方程式
2-acetyl-thiophene
ethyl heptafluorobutyrate
→
4,4,5,5,6,6,6-Heptafluoro-1-(2-thienyl)-1,3-hexanedione
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他The compound was synthesized
実験手順
The compound was synthesized according to example 1 using 2-acetyl-thiophene and ethyl heptafluorobutyrate as starting materials. 1H NMR (CDCl3): 6.49 (s, 1 H); 7.21 (dd, 1 H, J=3.8 & 5.1); 7.77 (dd, 1 H, J=1.2 & 5.1 Hz); 7.85 (dd, 1 H, J=1.2 & 3.8 Hz). IR (film): 1589 (C═O); 1230 (C—F).