反応 #1399

反応方程式

4,4'-difluorodiphenylmethane

water

→

4,4'-difluorobenzophenone

収率 95.0%

反応条件

後処理

1. 1
   その他20 g off-white solids, after toluene removal

実験手順

The procedure of Example 1 was used except that 20 g 4,4'-difluorodiphenylmethane, 30 g water, 31 g MnO2 and 50 g H2 SO4 were used. 20 g off-white solids, after toluene removal, afforded 95% pure 4,4'-difluorobenzophenone in a 90% yield.

出典