反応 #1369946
ord-8c602bc9aeed4c2b81685d0fc6f606aa
反応方程式
carbamic acid chloride
1-phenylsulfonyl-1,3-diaza-cyclohexane-2-one
phosgene
→
1-Chlorocarbonyl-2-oxo-3-phenylsulfonyl-1,3-diaza-cyclohexane
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他The product was recrystallized from acetone/petrolether
実験手順
This carbamic acid chloride was produced as described in Example 27 A from 6 parts by weight of 1-phenylsulfonyl-1,3-diaza-cyclohexane-2-one and 5 parts by weight of phosgene. The product was recrystallized from acetone/petrolether.