反応 #1369

反応方程式

2-methyl-3,4,6-trifluorobenzoic acid

chloride

→

2-methyl-3,4,6-trifluorobenzoyl chloride

反応条件

後処理

1. 1
   温度the mixture is refluxed for 1 hour
2. 2
   濃縮After concentrating

実験手順

To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for 1 hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.

出典