反応 #1365706

ord-8df9a23df07745eab43ba41bd6dfb9e9

反応方程式

COc1ccc(C=O)cc1
Anisaldehyde
CC(=O)O
acetic acid
O=S(=O)(O)O
sulfuric acid
COc1ccc(C=O)cc1.O=S(=O)(O)O
Anisaldehyde sulfuric acid

溶媒

反応条件

温度
100°CELSIUS
詳細条件
See reaction.notes.procedure_details.

実験手順

Anisaldehyde (0.5 ml) is mixed with glacial acetic acid (10 ml), methanol (85 ml) and concentrated sulfuric acid (5 ml). This solution is sprayed onto the TLC plate, which is then heated at 100° C.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06444233B1uspto-grants-2002_09