反応 #1356017

ord-5c19de62a33e4d3c89de8f17995b00f5

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

19 was prepared from 4-amino-2-bromo-thieno[3,2-c]pyridine-7-carboxylic acid amide 17 and 4-methyl-2-thiopheneboronic acid according to the general procedure described in Example 2. 1H NMR (400 MHz, d6-DMSO) δ: 2.25 (s, 3H), 7.29 (s, 1H), 7.36 (s, 1H), 7.80 (br s, 1H), 8.14 (s, 1H), 8.40 (br s, 1H), 8.46 (s, 1H). MS (EI) m/z (M+H+) 290.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07199119B2uspto-grants-2007_04